Basic 1h And 13c Nmr Spectroscopy

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Author: Metin Balci
Publisher: Elsevier
ISBN: 9780080525532
Size: 68.14 MB
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Basic 1h And 13c Nmr Spectroscopy by Metin Balci

Original Title: Basic 1h And 13c Nmr Spectroscopy

Nuclear Magnetic Resonance (NMR) spectroscopy is a powerful and theoretically complex analytical tool. Basic 1H- and 13C-NMR Spectroscopy provides an introduction to the principles and applications of NMR spectroscopy. Whilst looking at the problems students encounter when using NMR spectroscopy, the author avoids the complicated mathematics that are applied within the field. Providing a rational description of the NMR phenomenon, this book is easy to read and is suitable for the undergraduate and graduate student in chemistry. Describes the fundamental principles of the pulse NMR experiment and 2D NMR spectra Easy to read and written with the undergraduate and graduate chemistry student in mind Provides a rational description of NMR spectroscopy without complicated mathematics

Tables Of Spectral Data For Structure Determination Of Organic Compounds

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Author: Ernö Pretsch
Publisher: Springer Science & Business Media
ISBN: 3662224550
Size: 18.94 MB
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Tables Of Spectral Data For Structure Determination Of Organic Compounds by Ernö Pretsch

Original Title: Tables Of Spectral Data For Structure Determination Of Organic Compounds

Although numerical data are, in principle, universal, the compilations presented in this book are extensively annotated and interleaved with text. This translation of the second German edition has been prepared to facilitate the use of this work, with all its valuable detail, by the large community of English-speaking scientists. Translation has also provided an opportunity to correct and revise the text, and to update the nomenclature. Fortunately, spectroscopic data and their relationship with structure do not change much with time so one can predict that this book will, for a long period of time, continue to be very useful to organic chemists involved in the identification of organic compounds or the elucidation of their structure. Klaus Biemann Cambridge, MA, April 1983 Preface to the First German Edition Making use of the information provided by various spectroscopic tech niques has become a matter of routine for the analytically oriented organic chemist. Those who have graduated recently received extensive training in these techniques as part of the curriculum while their older colleagues learned to use these methods by necessity. One can, therefore, assume that chemists are well versed in the proper choice of the methods suitable for the solution of a particular problem and to translate the experimental data into structural information.

Basic One And Two Dimensional Nmr Spectroscopy

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Author: Horst Friebolin
Publisher: Wiley-VCH
ISBN: 9783527290598
Size: 78.25 MB
Format: PDF
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Basic One And Two Dimensional Nmr Spectroscopy by Horst Friebolin

Original Title: Basic One And Two Dimensional Nmr Spectroscopy

With a foreword by J. D. Roberts Written by an NMR expert with long-standing teaching experience, the first edition of this textbook has been a huge success. New features of this thoroughly revised and substantially enlarged second edition include * NMR spectroscopy of nuclides other than 1H and 13C * 'reverse' procedures for recording spectra Chemists, biologists, physicians, pharmacists and technical assistants will find this new edition even more useful for their daily work. From reviews of the first edition: 'This book is a pleasure to read and if it does not arouse the student's interest, then it is difficult to see what could. It is clearly written and illustrated ... good value and essential reading for anyone wanting to know more about NMR.' Chemistry in Britain 'Another paperback that I would advise students to buy ... [it] can be recommended for general purchase by all chemists.' New Scientist

Crc Handbook Of Basic Tables For Chemical Analysis Third Edition

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Author: Thomas J. Bruno
Publisher: CRC Press
ISBN: 9781420080438
Size: 21.87 MB
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Crc Handbook Of Basic Tables For Chemical Analysis Third Edition by Thomas J. Bruno

Original Title: Crc Handbook Of Basic Tables For Chemical Analysis Third Edition

Winner of an Oustanding Academic Title Award for 2011! Researchers in organic chemistry, chemical engineering, pharmaceutical science, forensics, and environmental science make routine use of chemical analysis, but the information these researchers need is often scattered in different sources and difficult to access. The CRC Handbook of Basic Tables for Chemical Analysis, Third Edition is a one-stop reference that presents updated data in a handy format specifically designed for use when reaching a decision point in designing an analysis or interpreting results. In response to a decade of reader input, this new edition has been expanded to include even more of the critical information scientists rely on to perform accurate analysis. Enhancements to the Third Edition: Includes data from the CRC Handbook of Fundamental Spectroscopic Correlation Charts into this volume for the first time Presents new information on gas, liquid, and thin layer chromatography; nuclear magnetic resonance spectrometry; infrared spectrophotometry; and mass spectrometry Reviews the detection of outliers in experimental data Provides basic information on thermocouples, chemical indicators, and chromatographic column regeneration Explores the latest stationary phases for chromatographic methods and extractions Examines carcinogens and chemical, electrical, radiation, and laser hazards Includes information on laboratory safety and equipment, from advice on choosing lab gloves and apparel to selecting respirators Unmatched in its coverage of the range of information scientists need in the lab, this resource will be referred to again and again by practitioners who need quick, easy access to the data that forms the basis for experimentation and analysis.

Organic Structures From Spectra

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Author: L. D. Field
Publisher: John Wiley & Sons
ISBN: 1118325486
Size: 80.61 MB
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Organic Structures From Spectra by L. D. Field

Original Title: Organic Structures From Spectra

The derivation of structural information from spectroscopic data is now an integral part of organic chemistry courses at all Universities. A critical part of any such course is a suitable set of problems to develop the student’s understanding of how structures are determined from spectra. Organic Structures from Spectra, Fifth Edition is a carefully chosen set of more than 280 structural problems employing the major modern spectroscopic techniques, a selection of 27 problems using 2D-NMR spectroscopy, more than 20 problems specifically dealing with the interpretation of spin-spin coupling in proton NMR spectra and 8 problems based on the quantitative analysis of mixtures using proton and carbon NMR spectroscopy. All of the problems are graded to develop and consolidate the student’s understanding of organic spectroscopy. The accompanying text is descriptive and only explains the underlying theory at a level which is sufficient to tackle the problems. The text includes condensed tables of characteristic spectral properties covering the frequently encountered functional groups. The examples themselves have been selected to include all important common structural features found in organic compounds and to emphasise connectivity arguments. Many of the compounds were synthesised specifically for this purpose. There are many more easy problems, to build confidence and demonstrate basic principles, than in other collections. The fifth edition of this popular textbook: • includes more than 250 new spectra and more than 25 completely new problems; • now incorporates an expanded suite of new problems dealing with the analysis of 2D NMR spectra (COSY, C H Correlation spectroscopy, HMBC, NOESY and TOCSY); • has been expanded and updated to reflect the new developments in NMR and to retire older techniques that are no longer in common use; • provides a set of problems dealing specifically with the quantitative analysis of mixtures using NMR spectroscopy; • features proton NMR spectra obtained at 200, 400 and 600 MHz and 13C NMR spectra include DEPT experiments as well as proton-coupled experiments; • contains 6 problems in the style of the experimental section of a research paper and two examples of fully worked solutions. Organic Structures from Spectra, Fifth Edition will prove invaluable for students of Chemistry, Pharmacy and Biochemistry taking a first course in Organic Chemistry. Contents Preface Introduction Ultraviolet Spectroscopy Infrared Spectroscopy Mass Spectrometry Nuclear Magnetic Resonance Spectroscopy 2DNMR Problems Index Reviews from earlier editions “Your book is becoming one of the “go to” books for teaching structure determination here in the States. Great work!” “…I would definitely state that this book is the most useful aid to basic organic spectroscopy teaching in existence and I would strongly recommend every instructor in this area to use it either as a source of examples or as a class textbook”. Magnetic Resonance in Chemistry “Over the past year I have trained many students using problems in your book - they initially find it as a task. But after doing 3-4 problems with all their brains activities... working out the rest of the problems become a mania. They get addicted to the problem solving and every time they solve a problem by themselves, their confident level also increases.” “I am teaching the fundamentals of Molecular Spectroscopy and your books represent excellent sources of spectroscopic problems for students.”

Carbon 13 Nmr Spectroscopy

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Author: J Stothers
Publisher: Elsevier
ISBN: 0323145507
Size: 73.24 MB
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Carbon 13 Nmr Spectroscopy by J Stothers

Original Title: Carbon 13 Nmr Spectroscopy

Carbon-13 NMR Spectroscopy focuses on the potential of 13C techniques and the practical difficulties associated with the detection of 13C NMR absorption. This monograph includes a descriptive presentation of 13C shielding results that has been adopted with emphasis on the structural and stereochemical aspects. Organized into four parts encompassing 11 chapters, this book starts with an overview of the characteristics of the NMR signals derived from compounds containing 13C nuclei in natural abundance that are inherently much weaker than those exhibited by protons. This monograph then compares the primary characteristics of 13C NMR with the more familiar proton methods. Other chapters consider the 13C spectra of pyridine, pyridazine, pyrimidine, pyrazine, s-triazine, and s-tetrazine. The final chapter deals with the effects of solute–solvent interactions on the shieldings of other nuclei. This monograph is intended for organic chemists, graduate students, and researchers in various branches of chemistry with an interest in 13C NMR methods as another approach to chemical problems.

Organic Structure Determination Using 2 D Nmr Spectroscopy

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Author: Jeffrey H. Simpson
Publisher: Academic Press
ISBN: 0123849705
Size: 33.63 MB
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Organic Structure Determination Using 2 D Nmr Spectroscopy by Jeffrey H. Simpson

Original Title: Organic Structure Determination Using 2 D Nmr Spectroscopy

"The second edition of this book comes with a number of new figures, passages, and problems. Increasing the number of figures from 290 to 448 has necessarily added considerable length, weight, and, expense. It is my hope that the book has not lost any of its readability and accessibility. I firmly believe that most of the concepts needed to learn organic structure determination using nuclear magnetic resonance spectroscopy do not require an extensive mathematical background. It is my hope that the manner in which the material contained in this book is presented both reflects and validates this belief"--

Nmr Spectroscopy Explained

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Author: Neil E. Jacobsen
Publisher: John Wiley & Sons
ISBN: 9780470173343
Size: 32.25 MB
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Nmr Spectroscopy Explained by Neil E. Jacobsen

Original Title: Nmr Spectroscopy Explained

NMR Spectroscopy Explained : Simplified Theory, Applications and Examples for Organic Chemistry and Structural Biology provides a fresh, practical guide to NMR for both students and practitioners, in a clearly written and non-mathematical format. It gives the reader an intermediate level theoretical basis for understanding laboratory applications, developing concepts gradually within the context of examples and useful experiments. Introduces students to modern NMR as applied to analysis of organic compounds. Presents material in a clear, conversational style that is appealing to students. Contains comprehensive coverage of how NMR experiments actually work. Combines basic ideas with practical implementation of the spectrometer. Provides an intermediate level theoretical basis for understanding laboratory experiments. Develops concepts gradually within the context of examples and useful experiments. Introduces the product operator formalism after introducing the simpler (but limited) vector model.

High Resolution Nmr Techniques In Organic Chemistry

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Author: Timothy D. W. Claridge
Publisher: Newnes
ISBN: 0080546285
Size: 73.47 MB
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High Resolution Nmr Techniques In Organic Chemistry by Timothy D. W. Claridge

Original Title: High Resolution Nmr Techniques In Organic Chemistry

"Nuclear Magnetic Resonance (NMR) Spectroscopy remains the foremost analytical technique for the structure elucidation of organic molecules and an indispensable tool for the synthetic, medicinal and natural product chemist. New techniques continue to emerge and the application of NMR methods continues to expand. High-Resolution NMR Techniques in Organic Chemistry is designed for use in academic and industrial NMR facilities, as a text for graduate-level NMR courses, and as an accessible reference for the chemist's or spectroscopist's desk." --Book Jacket.

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